Diastereoselective synthesis of (2S,5R)-5-hydroxypipecolic acid and 6-substituted derivatives.
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SourceOrganic Letters, 6, 26, (2004), pp. 4941-4
Article / Letter to editor
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Solid State Chemistry
Synthetic Organic Chemistry
SubjectMolecular Materials; Synthetic Organic Chemistry
[reaction: see text] Herein, we report a diastereoselective synthesis of the natural product (2S,5R)-5-hydroxypipecolic acid and 6-substituted derivatives thereof. The key step in the synthetic sequence is a novel highly diastereoselective epoxidation reaction of an enantiomerically pure cyclic enamide intermediate.
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